差示扫描量热法
钛镍合金
材料科学
高原(数学)
统计分析
拉伸试验
极限抗拉强度
统计显著性
冶金
数学
统计
形状记忆合金
热力学
物理
数学分析
作者
Ariane Salgado Gonzaga,David Salgado GONZAGA,Hallissa Simplício Gomes Pereira,Renato Parsekian Martins,Marília Regalado Galvão,Sergei Godeiro Fernandes Rabelo Caldas
标识
DOI:10.1590/2177-6709.26.2.e211945.oar
摘要
ABSTRACT Objective: This paper aims to verify the thermodynamic, mechanical and chemical properties of CuNiTi 35ºC commercial wires. Methods: Forty pre-contoured copper-nickel-titanium thermodynamic 0.017 x 0.025-in archwires with an Af temperature of 35°C were used. Eight wires from five different manufacturers (American Orthodontics® [G1], Eurodonto® [G2], Morelli® [G3], Ormco® [G4] and Orthometric® [G5]) underwent cross-sectional dimension measurements, tensile tests, SEM-EDS and differential scanning calorimetry (DSC) tests. Parametric tests (One-way ANOVA and Tukey post-test) were used, with a significance level of 5%, and Pearson’s correlation coefficient test was performed between the Af and chemical elements of the wires. All sample tests and statistical analyses were double-blinded. Results: All wires presented standard dimensions (0.017 x 0.025-in) and superelastic behavior, with mean plateau forces of: G1 = 36.49N; G2 = 27.34N; G3 = 19.24 N; G4 = 37.54 N; and G5 = 17.87N. The Af means were: G1 = 29.40°C, G2 = 29.13°C and G3 = 31.43°C, with p>0.05 relative to each other. G4 (32.77°C) and G5 (35.17°C) presented statistically significant differences between each other and among the other groups. All samples presented Ni, Ti, Cu and Al in different concentrations. Conclusions: The chemical concentration of the elements that compose the alloy significantly influenced the thermodynamic and mechanical properties.
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