正交晶系
拉曼光谱
材料科学
复合数
X射线光电子能谱
热液循环
纳米结构
比表面积
打赌理论
化学工程
分析化学(期刊)
水热合成
纳米技术
晶体结构
复合材料
化学
结晶学
色谱法
有机化学
催化作用
工程类
物理
光学
作者
Bapuso M. Babar,Suhas H. Sutar,S.H. Mujawar,Suraj Patil,Umesh D. Babar,Udayraj T. Pawar,Prakash M. Kadam,P.S. Patil,L.D. Kadam
标识
DOI:10.1016/j.mseb.2023.116827
摘要
Current study displays an actual hydrothermal synthesis of V2O5-rGO composite and further investigates how changes in rGO composition in V2O5-rGO composites affected their NO2 sensing property. The orthorhombic crystal structure is confirmed by XRD and Raman techniques, and the optimum proportion of disorders in the composite as a result of rGO is also confirmed. Porous nanostructure is observed in SEM images. The C, V, and O present in the composite are confirmed by the XPS results, along with a fluctuation in V4+/V5+. The BET technique was used to measure specific surface area (25.91 m2g−1) and pore radius (6.4140 nm). A prominent PL peak confirm presence of oxygen vacancies. At 150 °C, gas sensing for 100 ppm concentration of NO2 gas revealed improved response about 121.85%. The calculated response/ recovery time for sample consisting 10 mg rGO are 39 and 262 s, respectively. Along with response, sample C shows excellent reproducibility and good stability.
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