丙酮
材料科学
X射线光电子能谱
共沉淀
纳米复合材料
检出限
化学工程
表面改性
催化作用
纳米技术
选择性
纳米颗粒
化学
有机化学
色谱法
工程类
作者
Ziyan Wang,Xueli Yang,Caixuan Sun,Hongyan Liu,Junkai Shao,Mengjie Wang,Junyi Dong,Guanlong Cao,Guofeng Pan
出处
期刊:Sensor Review
[Emerald (MCB UP)]
日期:2022-10-12
卷期号:42 (6): 638-647
被引量:6
标识
DOI:10.1108/sr-12-2021-0486
摘要
Purpose This paper aims to successfully synthesize three-dimensional spindle-like Au functionalized Co 3 O 4 -ZnO nanocomposites; characterize the structure, morphology and surface chemical properties of the products; study the effect of Au NPs doping concentration, operating temperature different gas to, sensing properties; and introduce an attractive gas sensor for acetone detection. Design/methodology/approach Au NPs functionalized Co 3 O 4 -ZnO nanocomposite was prepared by coprecipitation and impregnation methods; the structure and surface chemical property of the products were characterized by XRD, SEM, TEM, UV-Vis, BET and XPS. The sensing ability of Au@Co 3 O 4 -ZnO for acetone and mechanism was analyzed systematically. Findings The results of gas sensing tests show that the unique component structure, Schottky junction and catalytic effect of Au functionalization make it have low operating temperature, excellent selectivity, high response (10 ppm, 56) and rapid response recovery time. Research limitations/implications All the characterization and test data of the prepared materials are provided in this paper and reveals the gas sensing mechanism of the gas sensor. Practical implications The detection limit is 2.92–100 ppb acetone. It is promising to be applied in low-power, micro detection and miniature acetone gas sensors. Social implications The gas sensor prepared has a lower working temperature and low detection limit, so it has promising application prospects in low-concentration acetone detection and early warning. Originality/value The unique component structure, Schottky junction and catalytic effect of Au functionalization Co 3 O 4 -ZnO make it have low operating temperature, excellent selectivity and rapid response recovery time.
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