石墨烯
单层
材料科学
拉曼光谱
透射电子显微镜
电子能量损失谱
电子
分析化学(期刊)
光电子学
纳米技术
光学
化学
物理
量子力学
色谱法
作者
Alice Apponi,Domenica Convertino,Neeraj Mishra,Camilla Coletti,M. Iodice,F. Frasconi,F. Pilo,Narcis Silviu Blaj,Daniele Paoloni,Ilaria Rago,Giovanni De Bellis,G. Cavoto,A. Ruocco
出处
期刊:Carbon
[Elsevier]
日期:2023-10-06
卷期号:216: 118502-118502
被引量:7
标识
DOI:10.1016/j.carbon.2023.118502
摘要
Here, we report on accurate transmission measurements of electrons below 1 keV through suspended monolayer graphene. Monolayer graphene was grown via chemical vapor deposition and transferred onto transmission electron microscopy (TEM) grids. A monochromatic electron gun has been employed to perform the measurements in the 30 – 900 eV range in ultra-high vacuum. The graphene transparency is obtained from the absolute measurement of the direct beam current and the transmitted one, by means of a Faraday cup. We observed a transmission going from 20 to 80% for monolayer graphene within the experimental electron energy range. The high quality and the grid coverage of the suspended graphene has been proved via micro-Raman, X-ray photoemission, electron energy loss spectroscopies and field-emission scanning electron microscopy. After a 550 °C in-vacuum annealing of the samples, the main contribution to the C 1s spectrum is due to the component and the evidence of suspended monolayer graphene has been observed through the -plasmon excitation.
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