扫描电子显微镜
多孔性
材料科学
微观结构
涂层
模拟体液
化学工程
复合材料
选择性激光熔化
沉浸式(数学)
电解质
电极
化学
几何学
数学
物理化学
工程类
作者
Ying Lv,Jiawei Guo,Weimin Huang,Yaojie Liu,Wentao Li,Guijiang Wei
出处
期刊:Anti-corrosion Methods and Materials
[Emerald (MCB UP)]
日期:2022-09-23
卷期号:69 (6): 660-666
被引量:6
标识
DOI:10.1108/acmm-08-2022-2684
摘要
Purpose The purpose of this paper is to improve the bioactivity of variable gradient TC4 porous scaffolds prepared by selective laser melting (SLM) through the micro-arc oxidation (MAO) technique. Design/methodology/approach Variable gradient TC4 porous scaffolds were prepared by SLM, then treated with MAO at different oxidation voltages. The microstructure, thickness and composition of MAO coatings were characterized by scanning electron microscope (SEM), energy-dispersive spectroscopy (EDS) and X-ray diffraction. The bioactivity of the MAO coatings was tested by simulated body fluid (SBF) immersion test. Findings SEM and EDS results show that with the increase of oxidation voltage, the content of Ca and P elements and the thickness of the MAO coatings increases. The thickness of the coating inside the scaffold is smaller than that of the outside regions. SBF immersion experiments showed that MAO-treated TC4 porous scaffolds had highest bioactivity at 440 V. Originality/value The variable gradient porous scaffolds were treated with MAO in the electrolyte containing Ca and P elements for the first time. The effect of oxidation voltages on the different region of porous scaffolds was studied in detail.
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