磷酸
活性炭
滴定法
化学
碳纤维
零电荷点
产量(工程)
微波食品加热
核化学
无机化学
X射线光电子能谱
傅里叶变换红外光谱
吸附
材料科学
有机化学
化学工程
复合数
工程类
复合材料
物理
量子力学
冶金
作者
Qing-Song Liu,Tao Zheng,Peng Wang,Liang Guo
标识
DOI:10.1016/j.indcrop.2009.10.011
摘要
Bamboo-based activated carbon was prepared with a microwave-induced activation process using phosphoric acid as the activating agent. The effects of various factors such as microwave power, radiation time and phosphoric acid/carbon ratio on the activation have been studied. The optimal activation conditions were determined as: microwave power 350 W, radiation time 20 min and phosphoric acid/carbon ratio 1:1, under which a surface area of 1432 m2/g and a carbon yield of 48% could be reached. The surface chemical properties were characterized with several methods including acid–base titration, point of zero charge (pHpzc) measurement, FTIR spectra and XPS spectra. The results demonstrated the existence of a large amount of acidic groups on the carbon surface, and the species and relative contents of these groups were analyzed in detail. Comparisons with the conventional thermal process demonstrated that the microwave-induced activation process had faster activation rate and higher carbon yield.
科研通智能强力驱动
Strongly Powered by AbleSci AI