热重分析
傅里叶变换红外光谱
热稳定性
材料科学
差热分析
磺酸
Crystal(编程语言)
单晶
差示扫描量热法
分析化学(期刊)
红外线的
蒸发
表征(材料科学)
热分析
晶体生长
热的
化学
结晶学
光学
有机化学
高分子化学
衍射
纳米技术
热力学
物理
计算机科学
程序设计语言
作者
K. Gayathiridevi,G. Pasupathi,B. Deepa,K. Kaviyarasu,A. Ayeshamariam
标识
DOI:10.1080/24701556.2022.2034001
摘要
We report the growth and characterization of 3-Amino benzene sulfonic acid (3-ABSA) of an organic single crystal for the first time under slow evaporation technique. The presence of characteristics vibrational groups and molecular structure were established by Fourier transform infrared (FTIR) and nuclear magnetic resonance (NMR) studies. The lower ultraviolet ray absorption edge was found to be 220 nm with a broad transmission window was observed in the visible region. The mechanical strength of grown crystal was assessed, and it belongs to soft material category. However, high thermal stability and other thermodynamic parameters were calculated using thermogravimetric (TGA) and differential thermal analyses (DTA). Therefore, the dielectric behavior of grown crystal was measured at various frequencies and temperature. The Kurtz powder second harmonic generation displays the second harmonic generation behavior of material and its efficiency is 0.55 times that of KDP were discussed in detail.
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