石墨烯
材料科学
尼古丁
拉曼光谱
检出限
再现性
纳米复合材料
扫描电子显微镜
氧化物
复合材料
纳米技术
化学
色谱法
冶金
医学
光学
物理
内科学
作者
Yue Zou,Lin Wang,Gang Xiao,Qi Zhang,Shuo Duan,Hongxun Wang,Xiaodan Liu,Jiahua Wang,Houde Dai,Huiying Zhou
标识
DOI:10.1016/j.jiec.2023.11.064
摘要
Electronic cigarettes (e-cigarette) have become more and more popular among young smokers in recent years. Nicotine, the main addictive component in cigarettes, is widely present in many e-cigarette. Assessing levels of nicotine is critical to the health of consumers and the development of tobacco industry. Herein, a novel electrochemical sensor based on Ag/TiO2 nanoparticles, metal–organic frameworks (MOFs) and graphene oxide (dual−NPs@HKUST−1/GO) nanocomposite was prepared for the rapid detection of nicotine in e-cigarette. The composites were characterized by scanning electron microscopy, X-ray diffraction, Raman spectroscopy and Fourier transform infrared spectroscopy, respectively. The results showed that the successfully synthesized composites have an average size of (20 ± 5) μm and excellent characterization properties. Under optimized conditions, the peak current response of nicotine with the differential pulse voltammetry showed a linear relationship in the range of 0.025–300 μM with a detection limit of 0.0145 μM. This newly developed dual−NPs@HKUST−1/GO-based sensor exhibited excellent selectivity, sensitivity and reproducibility for the accurate detection of nicotine. In addition, it also has excellent performance in detecting nicotine in actual e-cigarette refill liquids. The recoveries ranged from 88.6 % to 101.8 % in e-cigarette refill liquids, indicating good detection performance. This method provides a new concept for the detection of nicotine in the tobacco industry and clinical fields.
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