Sesquiterpenoids from Streptomyces anulatus isolated from Giraffa camelopardalis feces

化学 异核单量子相干光谱 质子核磁共振 碳-13核磁共振 二维核磁共振波谱 光谱(功能分析) 碳-13核磁共振卫星 立体化学 核磁共振波谱 核磁共振 氟-19核磁共振 物理 量子力学
作者
Nan Ding,Li Han,Yi Jiang,Gui-Ding Li,Jiang Liu,Yu Mu,Xueshi Huang
出处
期刊:Magnetic Resonance in Chemistry [Wiley]
卷期号:56 (5): 352-359 被引量:13
标识
DOI:10.1002/mrc.4709
摘要

Table S1. 1H NMR (600 MHz) and 13C NMR (150 MHz) data for compounds 8–10 in DMSO-d6 Table S2. 1H NMR (600 MHz) and 13C NMR (150 MHz) data for compounds 11–13 Table S3. Comparison of 13C NMR data for compounds 4, 8–13 with the literature Figure S1. 1H NMR (600 MHz, DMSO-d6) spectrum of compound 1 Figure S2. 1H NMR (600 MHz, DMSO-d6) spectrum of compound 1-expanded Figure S3. 13C NMR (150 MHz, DMSO-d6) spectrum of compound 1 Figure S4. HSQC spectrum of compound 1 Figure S5. HMBC spectrum of compound 1 Figure S6. COSY spectrum of compound 1 Figure S7. NOESY spectrum of compound 1 Figure S8. 1H NMR (600 MHz, DMSO-d6) spectrum of compound 2 Figure S9. 1H NMR (600 MHz, DMSO-d6) spectrum of compound 2-expanded Figure S10. 13C NMR (150 MHz, DMSO-d6) spectrum of compound 2 Figure S11. HSQC spectrum of compound 2 Figure S12. HMBC spectrum of compound 2 Figure S13. COSY spectrum of compound 2 Figure S14. NOESY spectrum of compound 2 Figure S15. 1H NMR (600 MHz, DMSO-d6) spectrum of compound 3 Figure S16. 1H NMR (600 MHz, DMSO-d6) spectrum of compound 3-expanded Figure S17. 13C NMR (150 MHz, DMSO-d6) spectrum of compound 3 Figure S18. HSQC spectrum of compound 3 Figure S19. HMBC spectrum of compound 3 Figure S20. COSY spectrum of compound 3 Figure S21. NOESY spectrum of compound 3 Figure S22. 1H NMR (600 MHz, DMSO-d6) spectrum of compound 5 Figure S23. 1H NMR (600 MHz, DMSO-d6) spectrum of compound 5-expanded Figure S24. 13C NMR (150 MHz, DMSO-d6) spectrum of compound 5 Figure S25. HSQC spectrum of compound 5 Figure S26. HMBC spectrum of compound 5 Figure S27. COSY spectrum of compound 5 Figure S28. NOESY spectrum of compound 5 Figure S29. 1H NMR (600 MHz, DMSO-d6) spectrum of compound 6 Figure S30. 1H NMR (600 MHz, DMSO-d6) spectrum of compound 6-expanded Figure S31. 13C NMR (150 MHz, DMSO-d6) spectrum of compound 6 Figure S32. HSQC spectrum of compound 6 Figure S33. HMBC spectrum of compound 6 Figure S34. COSY spectrum of compound 6 Figure S35. NOESY spectrum of compound 6 Figure S36. 1H NMR (600 MHz, DMSO-d6) spectrum of compound 7 Figure S37. 1H NMR (600 MHz, DMSO-d6) spectrum of compound 7-expanded Figure S38. 13C NMR (150 MHz, DMSO-d6) spectrum of compound 7 Figure S39. HSQC spectrum of compound 7 Figure S40. HMBC spectrum of compound 7 Figure S41. COSY spectrum of compound 7 Figure S42. NOESY spectrum of compound 7 Figure S43. 1H NMR (600 MHz, CDCl3) spectrum of compound 4 Figure S44. 13C NMR (150 MHz, CDCl3) spectrum of compound 4 Figure S45. 1H NMR (600 MHz, DMSO-d6) spectrum of compound 8 Figure S46. 1H NMR (600 MHz, DMSO-d6) spectrum of compound 8-expanded Figure S47. 13C NMR (150 MHz, DMSO-d6) spectrum of compound 8 Figure S48. HSQC spectrum of compound 8 Figure S49. HMBC spectrum of compound 8 Figure S50. COSY spectrum of compound 8 Figure S51. NOESY spectrum of compound 8 Figure S52. 1H NMR (600 MHz, DMSO-d6) spectrum of compound 9 Figure S53. 1H NMR (600 MHz, DMSO-d6) spectrum of compound 9-expanded Figure S54. 13C NMR (150 MHz, DMSO-d6) spectrum of compound 9 Figure S55. HSQC spectrum of compound 9 Figure S56. HMBC spectrum of compound 9 Figure S57. COSY spectrum of compound 9 Figure S58. NOESY spectrum of compound 9 Figure S59. 1H NMR (600 MHz, DMSO-d6) spectrum of compound 10 Figure S60. 1H NMR (600 MHz, DMSO-d6) spectrum of compound 10-expanded Figure S61. 13C NMR (150 MHz, DMSO-d6) spectrum of compound 10 Figure S62. HSQC spectrum of compound 10 Figure S63. HMBC spectrum of compound 10 Figure S64. COSY spectrum of compound 10 Figure S65. NOESY spectrum of compound 10 Figure S66. 1H NMR (600 MHz, DMSO-d6) spectrum of compound 11 Figure S67. 1H NMR (600 MHz, DMSO-d6) spectrum of compound 11-expanded Figure S68. 13C NMR (150 MHz, DMSO-d6) spectrum of compound 11 Figure S69. HSQC spectrum of compound 11 Figure S70. HMBC spectrum of compound 11 Figure S71. COSY spectrum of compound 11 Figure S72. NOESY spectrum of compound 11 Figure S73. 1H NMR (600 MHz, DMSO-d6) spectrum of compound 12 Figure S74. 1H NMR (600 MHz, DMSO-d6) spectrum of compound 12-expanded Figure S75. 13C NMR (150 MHz, DMSO-d6) spectrum of compound 12 Figure S76. HSQC spectrum of compound 12 Figure S77. HMBC spectrum of compound 12 Figure S78. COSY spectrum of compound 12 Figure S79. NOESY spectrum of compound 12 Figure S80. 1H NMR (600 MHz, DMSO-d6) spectrum of compound 13 Figure S81. 1H NMR (600 MHz, DMSO-d6) spectrum of compound 13-expanded Figure S82. 13C NMR (150 MHz, DMSO-d6) spectrum of compound 13 Figure S83. HSQC spectrum of compound 13 Figure S84. HMBC spectrum of compound 13 Figure S85. COSY spectrum of compound 13 Figure S86. NOESY spectrum of compound 13 Figure S87. 1H NMR (600 MHz, acetone-d6) spectrum of compound 13 Figure S88. 1H NMR (600 MHz, acetone-d6) spectrum of compound 13-expanded Figure S89. 13C NMR (150 MHz, acetone-d6) spectrum of compound 13 Figure S90. HSQC (acetone-d6) spectrum of compound 13 Figure S91. NOESY (acetone-d6) spectrum of compound 13 Please note: The publisher is not responsible for the content or functionality of any supporting information supplied by the authors. Any queries (other than missing content) should be directed to the corresponding author for the article.
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