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Preparation and Properties of Indium Ion Modified Graphite Felt Composite Electrode

石墨 材料科学 循环伏安法 电极 介电谱 电化学 化学工程 超级电容器 扫描电子显微镜 表面改性 复合材料 化学 工程类 物理化学
作者
Yang Su,Na Chen,Hai‐lin Ren,Lili Guo,Zhen Li,Xiaomin Wang
出处
期刊:Frontiers in Chemistry [Frontiers Media]
卷期号:10 被引量:18
标识
DOI:10.3389/fchem.2022.899287
摘要

Iron-chromium redox flow batteries (ICRFBs) have the advantages of high safety, long cycle life, flexible design, and low maintenance costs. Polyacrylonitrile-based graphite felt composite material has good temperature resistance, corrosion resistance, large surface area and excellent electrical conductivity, and is often used as the electrode material of ICRFB, but its chemical activity is poor. In order to improve the activity of the graphite felt electrode, In3+ was used for modification in this paper, and the modified graphite felt was used as the electrode material for iron-chromium batteries. The structure and surface morphology of the modified graphite felt were analyzed by the specific surface area analyzer and scanning electron microscope; the electrochemical impedance spectroscopy and cyclic voltammetry experiments were carried out on the electrochemical workstation to study the electro catalytic activity of In3+ modified graphite felt and its performance in ICRFBS. The results show that the graphite felt electrode modified with a concentration of 0.2 M In3+ was activated at 400°C for 2 h, and its surface showed a lot of grooves, and the specific surface area reached 3.889 m2/g, while the specific surface area of the untreated graphite felt was only 0.995 m2/g significantly improved. Electrochemical tests show that the electrochemical properties of graphite felt electrodes are improved after In3+ modification. Therefore, the In3+ modified graphite felt electrode can improve the performance of ICRFB battery, and also make it possible to realize the engineering application of ICRFB battery.
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