间苯二甲酸
材料科学
醇盐
金属有机骨架
金属
衍射
粉末衍射
化学工程
溶剂
纳米技术
结晶学
有机化学
冶金
化学
催化作用
复合材料
光学
吸附
工程类
物理
聚酯纤维
对苯二甲酸
作者
Omar Barreda,Gregory R. Lorzing,Eric D. Bloch
出处
期刊:Powder Diffraction
[Cambridge University Press]
日期:2019-04-11
卷期号:34 (2): 119-123
被引量:7
标识
DOI:10.1017/s0885715619000228
摘要
Powder X-ray diffraction was used to monitor the solvent-free synthesis of two-dimensional (2D) metal–organic frameworks (MOFs) via mechanochemical methods. For four isophthalic acid-based, alkoxide-functionalized organic ligands, optimal milling times were found to vary from 12 to 48 min. This work confirms that mechanochemical synthesis routes can be utilized to afford highly-crystalline, 2D MOFs.
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