Achieving outstanding mechanical/bonding performances by epoxy nanocomposite as concrete–steel rebar adhesive using silane modification of nano SiO2

硅烷 材料科学 胶粘剂 环氧树脂 复合材料 纳米复合材料 抗压强度 极限抗拉强度 纳米- 表面改性 粘附 纳米颗粒 化学工程 图层(电子) 纳米技术 工程类
作者
Reza Ghamarpoor,Masoud Jamshidi,Majid Mohammadpour
出处
期刊:Scientific Reports [Nature Portfolio]
卷期号:13 (1) 被引量:30
标识
DOI:10.1038/s41598-023-36462-0
摘要

Anchoring steel rebar in concrete structures is a common method in the building and construction industry. This research focuses on improving the mechanical/bonding properties of the prepared epoxy nanocomposite adhesive using surface treatment of SiO2 nano fillers by glycidoxypropyltrimethoxysilane (GPTMS). For this purpose, the nano silica particles were silanized via a facile sol-gel method at silane concentrations of 1, 5, 10 and 20X (i.e. X is stoichiometric silane concentration). The nanoparticles were characterized carefully by FTIR, TGA, XRD and XPS techniques. It was found that the highest GPTMS grafting ratio was obtained at silane concentration of 10X. The pure and silanized nanoparticles were added to a two-pack epoxy resin and were compared for tensile and compressive properties. It was found that surface modification of nano silica caused improvement in the strength, modulus, compressive strength and compressive modulus by 56, 81, 200 and 66% compared to the pristine epoxy adhesive and also 70, 20, 17 and 21% compared to the pure nano silica containing adhesive. It also caused 40 and 25% improvement in the pullout strength, 33 and 18% enhancement in the pullout displacement and 130 and 50% in adhesion energy compared to the pristine and raw silica-containing adhesives, respectively.

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