材料科学
热重分析
硅酸钠
复合材料
纳米颗粒
色散(光学)
涂层
扫描电子显微镜
氧化铁
磁性纳米粒子
化学工程
冶金
纳米技术
光学
物理
工程类
作者
Gustavo Tontini,Leandro Lima Evangelista,Antônio Itamar Ramos Filho,Rosa Angélica Elias,Gisele Hammes,Nelson Jhoe Batistela,Cristiano Binder,Aloı́sio Nelmo Klein,V. Drago
标识
DOI:10.1016/j.jmmm.2019.165351
摘要
This work presents the study and development of soft magnetic composites of iron coated with alumina nanoparticles dispersed in sodium silicate, also known as liquid glass. It is proposed that the nanoparticles dispersion increases the thermal resistance of the glassy coating, allowing a heat treatment with higher temperatures, reducing the internal stresses generated during the pressing and reducing core losses. Thermogravimetric analysis under an oxidative atmosphere of the powder samples and Scanning electron microscopy and energy-dispersive X-ray diffraction of fractured compacted samples are shown to discuss the coating thermal behavior. Also, electrical resistivity, relative permeability and magnetic losses of samples with and without nanoparticles dispersed in sodium silicate are shown discussing their loss separation.
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