化学
角鲨酸
酒
烷基
有机化学
原甲酸三乙酯
组合化学
催化作用
作者
Hiu Liu,Craig S. Tomooka,Harold W. Moore
标识
DOI:10.1080/00397919708006826
摘要
Abstract An efficient and general method for the synthesis of alkyl squarates is presented. This involves the reactions of squaric acid with the desired alcohol in the presence of an orthoformate. This was applicable for the synthesis of dimethyl-, diethyl-, diisopropyl, di-n-butyl and di-t-butyl squarates in yields ranging from 77–97%. It is a convenient and safe method that can be accomplished on a multigram scale.
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