膜
石墨烯
碳二亚胺
氧化物
化学
胺气处理
核化学
过滤(数学)
化学工程
海水淡化
傅里叶变换红外光谱
材料科学
高分子化学
纳米技术
有机化学
生物化学
统计
工程类
数学
作者
Parisa Sadat Parsamehr,Marzieh Zahed,Maryam Ahmadzadeh Tofighy,Toraj Mohammadi,Mashallah Rezakazemi
出处
期刊:Desalination
[Elsevier]
日期:2019-10-01
卷期号:468: 114079-114079
被引量:80
标识
DOI:10.1016/j.desal.2019.114079
摘要
A novel cross-linked graphene oxide (GO) membrane was prepared by vacuum filtration using a two-step method, including activation of GO carboxyl groups by a mixture of 1-Ethyl-3- (3-dimethylaminopropyl) carbodiimide (EDC) and N -Hydroxysuccinimide (NHS) and then cross-linking with polyethyleneimine (PEI). In the cross-linking process, the activated carboxyl groups of GO react with amine groups of PEI through a simple and efficient method. GO cross-linking with PEI significantly improves membrane dimensional stability and salt rejection. The rejection of the cross-linked GO membrane was evaluated by NaCl, Na2SO4 and MgCl2 solutions, and the obtained results followed the order of R (MgCl2) > R (NaCl) > R (Na2SO4). The prepared cross-linked GO membrane was characterized by FTIR, XRD, SEM, FESEM, EDS, WCA, AFM and BET analysis. Also, the effects of operating parameters such as N2 pressure, feed temperature and pH on the cross-linked GO membrane performance were investigated.
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