The effect of quenching/double quenching and tempering heat treatment cycles on the microstructure, impact energy and hardness of AISI H13 tool steel

In this study, microstructure modifications of AISI H13 steel were studied with different heat treatments such as conventional quenching, quenching + tempering/double tempering and double quenching + tempering/double tempering. Carbide volume ratio analyses were performed. The XRD analysis was used to determine the type of carbide, the average crystallite size, and the dislocation density in the samples. Charpy impact tests were performed. The hardness values of the samples were measured with the Rockwell C scale. The presence of MC, M23C6, and M7C3 type carbides was determined in the microstructures. Heat treatment cycles caused a high dislocation density in martensite laths. The dislocation density of martensite laths decreased with double quenching. The tempering process caused the formation of fine carbide particles in the microstructure. In addition, tempering processes gave rise to an increase in the volume ratio of M23C6-type strip carbides. The length/width ratio of the strip-type carbides increased with the effect of double tempering. As a result of the applied heat treatments, the impact energies of the samples decreased. The tempering process caused a secondary hardening of the samples. While the double quenching process increased the impact energy value by approximately 2%, it caused a decrease in hardness by 24%.