结晶度
热重分析
傅里叶变换红外光谱
角蛋白
材料科学
羊毛
萃取(化学)
化学工程
核化学
化学
复合材料
色谱法
有机化学
医学
工程类
病理
作者
Weidong Du,Liran Zhang,Changhuan Zhang,Jianjun Cao,Dongmin Wang,Hongwei Li,Wenxia Li,Jinling Zeng
标识
DOI:10.3389/fmats.2021.789081
摘要
Keratin is a plentiful and renewable fibrous protein resource found in nature, but a great deal of keratin-containing waste causes environmental problems, especially wool waste, which accounts for the majority. A green and efficient extraction method of keratin based on microwave induction method was studied. Compared with traditional thermal induction, the extraction time was shortened by half, and the dissolution rate of the wool was improved. The effects of the above two methods on the size, structure, crystallinity, and thermal stability of wool keratin were studied by a series of analysis methods [e.g., attenuated total reflectance Fourier transform infrared spectrometry (ATR-FTIR), Raman spectroscopy, X-ray diffraction spectroscopy (XRD), dynamic light scattering (DLS), thermogravimetric analysis (TG), and so on]. The results showed that under microwave irradiation, the disulfide bonds were destroyed greatly, and the secondary structure changed significantly, which was beneficial to obtain wool keratin with low crystallinity and small particle size.
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