拉曼光谱
X射线光电子能谱
表征(材料科学)
材料科学
电化学
显微镜
扫描电化学显微镜
光谱学
扫描电子显微镜
纳米技术
电感耦合等离子体质谱法
分析化学(期刊)
质谱法
化学工程
化学
电极
光学
物理化学
物理
工程类
量子力学
复合材料
色谱法
作者
Anaclet Nsabimana,Yiran Guan,Guobao Xu
摘要
The hydrogen evolution reaction is important in energy conversion and storage. This has led to the design of different types of catalysts and production setups. Understanding the status of the catalysts and reaction mechanisms motivated researchers to adopt the operando/in situ techniques. Herein, we present a brief overview of the recent (from 2020) advances in the use of in situ and operando characterization techniques, such as in situ X-ray absorption spectroscopy, X-ray photoelectron spectroscopy, X-ray diffraction analysis, IR spectroscopy, electrochemical Raman spectroscopy, online inductively coupled plasma - mass spectroscopy, differential electrochemical mass spectroscopy, optical microscopy, electron microscopy, electrochemical atomic microscopy, electrochemical scanning tunneling microscopy, and scanning electrochemical microscopy, in the electrochemical hydrogen evolution reaction. Representative examples of the applications of these techniques are also provided. Challenges in this field and future perspectives are discussed.
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