罗丹明B
铋
漫反射红外傅里叶变换
尿素
拉曼光谱
材料科学
光催化
扫描电子显微镜
微晶
光谱学
带隙
光降解
粒径
罗丹明
核化学
化学工程
化学
有机化学
光学
催化作用
复合材料
荧光
物理
光电子学
量子力学
冶金
工程类
作者
Viktória Márta,Zsolt Pap,Enikő Bárdos,Tamás Gyulavári,Gábor Veréb,Klára Hernádi
出处
期刊:Catalysts
[MDPI AG]
日期:2023-03-20
卷期号:13 (3): 616-616
标识
DOI:10.3390/catal13030616
摘要
Bismuth oxybromides were prepared via a solvothermal method by applying different urea amounts during synthesis. The effects of the urea ratio on the morpho–structural properties and photocatalytic activity of the samples were investigated. X-ray diffraction, diffuse reflectance spectroscopy, infrared spectroscopy, Raman spectroscopy, scanning electron microscopy, and surface tension measurements were carried out to characterize the samples. Their photoactivity was evaluated by the photocatalytic degradation of rhodamine B and ibuprofen under UV and visible light irradiations. The urea ratio notably influenced morphology, particle size distribution, and photoactivity. However, it only had a limited effect on the crystalline composition, primary crystallite size, and band gap of bismuth oxybromides. The formation of Bi-based complexes and degraded urea-based products were observed, which were deduced to influence band gap energies and hence, photoactivity. Predominantly, samples prepared at low urea ratios proved to be the best for both rhodamine B and ibuprofen degradations under both irradiations.
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