Evaluation of the Polyethylene Glycol Impregnation and Vacuum Freeze-Drying Method for Waterlogged Archaeological Wood: Conservation of the Yenikapı 1 Shipwreck

PEG比率 聚乙二醇 冷冻干燥 傅里叶变换红外光谱 材料科学 聚乙烯 复合材料 制浆造纸工业 核化学 化学 化学工程 色谱法 有机化学 财务 工程类 经济
作者
Namık Kılıç,Aslı Gökçe Kılıç
出处
期刊:Studies in Conservation [Taylor & Francis]
卷期号:69 (5): 336-347 被引量:4
标识
DOI:10.1080/00393630.2023.2235222
摘要

The YK 1 shipwreck, found at Yenikapı, Istanbul, is one of 37 shipwrecks dating to the medieval era. This paper describes the studies and the processes which were conducted to conserve the YK 1. Firstly, the level of physical and chemical degradation of the wood from the YK 1 was examined, which revealed that the wood was highly degraded. Therefore, PEG 2000 was chosen for the impregnation process before vacuum freeze-drying. In addition, the ASE values confirmed that the PEG 2000 impregnation and vacuum freeze-drying method together were successful in conserving the YK 1, with values higher than PEG 2000 impregnation and vacuum freeze-drying methods alone. The concentration of the PEG solution in the tank was monitored throughout the impregnation process. Following this, samples taken from the wood cores were analysed using FTIR to evaluate the effectiveness of the impregnation process. Finally, SEM was used to examine the effectiveness of the PEG 2000 impregnation and vacuum freeze-drying method. The SEM images showed that the PEG 2000 was uniformly distributed, and the wood had no deformation after freeze-drying.
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