材料科学
煅烧
纳米颗粒
透射电子显微镜
微观结构
化学工程
扫描电子显微镜
液化石油气
表征(材料科学)
氧化物
钨
氧气
纳米技术
相(物质)
复合材料
化学
冶金
有机化学
催化作用
工程类
作者
Subhash Singh,S. B. Majumder
摘要
Metal oxide sensors, such as ZnO, SnO2, and WO3 etc. have been utilized for several decades for low-costd etection of combustible and toxic gases. In the present work tungsten oxide (WO3) nanoparticles have been prepared by using an economic wet chemical synthesis route. To understand the phase formation behavior of the synthesized powders, X-ray diffraction analysis has been performed. The microstructure evolution of the synthesized powders was characterized by field-emission scanning electron microscopy (FESEM), and transmission electron microscopy (TEM). The calcined phase pure WO3 nanoparticles are investigated in terms of LPG gas sensing properties. The gas sensing measurements has been done in two different mode of operation (namely static and dynamic measurements). The degree of oxygen deficiency in the WO3 sensor also affected the sensor properties and the optimum oxygen content of WO3 was necessary to get high sensitivity for LPG. The WO3 sensor shows the excellent sensor properties for LPG at the operating temperature of 250°C.
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