铪
水合物
氢氧化物
材料科学
化学工程
无机化学
化学
冶金
有机化学
锆
工程类
作者
Ilya B. Polovov,Yakov S. Bataev,Yurii D. Afonin,Vladimir A. Volkovich,А. В. Чукин,Aydar Rakhmatullin,Miroslav Boča
标识
DOI:10.1016/j.jallcom.2019.03.103
摘要
Abstract A comprehensive study of processes taking place during synthesis and subsequent thermal treatment of hafnium oxide was performed. Synthesis of HfO2 involves following stages: stepwise dehydration of hydrated hafnium hydroxide, crystallization of metastable tetragonal phase of HfO2 and subsequent irreversible transition to the stable monoclinic modification. Preliminary heat treatment lowered temperature of crystallization of HfO2 and resulted in changing process mechanism.
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