正硅酸乙酯
材料科学
分散剂
溴化铵
聚乙二醇
纳米复合材料
傅里叶变换红外光谱
热分解
化学工程
表面改性
扫描电子显微镜
核化学
纳米技术
色散(光学)
复合材料
肺表面活性物质
有机化学
化学
光学
物理
工程类
作者
Viviana Daboin,Sarah Briceño,Jorge Suárez,Gema González
标识
DOI:10.1016/j.jmmm.2017.08.043
摘要
Cobalt ferrite nanoparticles CoFe2O4 were synthesized using the thermal decomposition method; subsequently the NPs were functionalized using poli vinyl pyrrolidone (PVP) cetyl trimethyl ammonium bromide (CTAB) and polyethylene glycol (PEG) as dispersing agent. Surface modification with silica SiO2 was made using the Stöber method and tetraethyl orthosilicate (TEOS) as precursor. The purpose of this study is to investigate the influence of the different dispersing agents on the structure and therefore on the magnetic properties of the CoFe2O4/SiO2 nanocomposites. Structural characterization was carried out using: X-ray diffraction (XRD), infrared spectroscopy (FTIR), transmission electron microscopy (TEM) and scanning electron microscopy (SEM). Magnetic properties were evaluated using a vibrating sample magnetometer (VSM) at room temperature. Our results revealed that the structural and magnetic properties of the CoFe2O4/SiO2 nanocomposites were significantly different depending of the type of dispersing agents used before the surface modification with silica SiO2.
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