Fundamentals of Fourier Transform Infrared Spectroscopy

Introduction to Infrared Spectroscopy Terms and Definitions The Properties of Light What Is an Infrared Spectrum? What Are Infrared Spectra Used For? The Advantages and Disadvantages of Infrared Spectroscopy The Advantages and Disadvantages of FTIR The Advantages of FTIRs The Disadvantage of FTIR FTIR: The Rest of the Story How an FTIR Works Interferometers and Interferograms How Many Scans Should Be Used? How an Interferogram Becomes a Spectrum Scanning Advice Instrumental Resolution What Determines Resolution in an FTIR Scan? What Resolution Should Be Used? FTIR Trading Rules FTIR Hardware Interferometers Infrared Sources Beamsplitters Infrared Detectors The Laser Testing Instrument Quality and Troubleshooting Proper Use of Spectral Processing The Rules of Spectral Processing Spectral Subtraction Subtraction Artifacts Baseline Correction Smoothing Spectral Derivatives Deconvolution Guidance, Precautions, and Limitations Spectral Library Searching The Search Process Interpreting Library Search Results Analysis of Mixtures: Subtract and Search Again Preparing Samples Properly Transmission Sampling Overview Windows, Cells, and Materials for Transmission Analysis Transmission Analysis of Solids and Powders KBr Pellets Mulls Transmission Analysis of Polymers The Cast Film Method The Heat and Pressure Method Transmission Analysis of Liquids Capillary Thin Films Sealed Liquid Cells Transmission Analysis of Gases and Vapors Reflectance Analysis Different Types of Reflectance Advantages and Disadvantages of Reflectance Sampling Specular Reflectance Diffuse Reflectance (DRIFTS) Abrasive Sampling Attenuated Total Reflectance (ATR) Depth of Penetration Applications of ATR Liquids Semi-Solids Polymers Powders ATR: Advantages and Disadvantages FTIR Sample Preparation: Overview and Recommendations Quantitative Infrared Spectroscopy Terms and Definitions Beer's Law Calibration and Prediction with Beer's Law Calibration Prediction An Experimental Protocol for Single Component Analyses Measuring Absorbances Properly Peak Areas versus Peak Heights Dealing with Overlapped Peaks Avoiding Experimental Errors Infrared Microscopy Hyphenated Infrared Techniques Infrared Microscopy Instrumentation Sample Preparation Applications Infrared Mapping and Imaging Glossary Index