材料科学
煅烧
扫描电子显微镜
热重分析
颗粒
锶
碳酸锶
粉末衍射
粒子(生态学)
粒径
化学工程
六方晶系
形态学(生物学)
矿物学
分析化学(期刊)
核化学
结晶学
复合材料
化学
色谱法
催化作用
地质学
工程类
有机化学
海洋学
生物
生物化学
遗传学
作者
S. Kanagesan,S. Jesurani,V. Ramachandran,T. Kalaivani
标识
DOI:10.1080/0371750x.2010.11090837
摘要
Strontium hexaferrite (SrFe12O19) powder was synthesized by sol-gel based combustion technique. In this technique, strontium and iron nitrates were used as the source nitrates and D-fructose as the fuel. The phase formation, thermal properties, particle morphology and surface morphology of the sintered pellets were analyzed by X-ray diffraction (XRD), thermogravimetry/differential thermal analysis (TG-DTA) and high-resolution scanning electron microscope (HR-SEM). Crystalline particles obtained by the calcinations of the precursor powder at 900°C, showed the crystalline diffraction pattern with the corresponding major angles, 30.41°, 31.02°, 32.37°, 34.24°, 35.81°, 37.21°, 40.47° and 42.60° respectively. HR-SEM studies have revealed that the structure of calcined particles is a mixed hexagonal and nearly plate like hexagonal, and the surface of the sintered pellets results in hexagonal structure with good magnetic properties.
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