Phenomenological sintering model and experimental validation of gravity-induced distortions in binder-jetted stainless steel components

烧结 材料科学 铁氧体(磁铁) 各向同性 复合材料 绿色车身 粘度 冶金 量子力学 物理
作者
Alberto Cabo Rios,Mats Persson,Eduard Hryha,Eugene A. Olevsky
出处
期刊:Ceramics International [Elsevier]
卷期号:50 (19): 37268-37281 被引量:12
标识
DOI:10.1016/j.ceramint.2024.04.427
摘要

Sintering is an important consolidation step employed in sinter-based metal additive manufacturing processes. Binder Jetting (BJT) starts with green components with low green density (40–60 %) that results in large sintering shrinkages and geometrical shape distortions caused by external forces (e.g. gravity). Consequently, the prediction of the final sintered geometry is crucial during the design process. In this work, a novel sintering simulation framework for gravity-affected sintering of stainless-steel components is presented, including the Rios-Olevsky-Hryha sintering model and the methodology for the identification of the required material parameters. The constitutive law includes material constants to account for the powder packing effects and the delta-ferrite transformation occurring at high temperatures. The material shear viscosity was explicitly related to the equilibrium phase fraction of austenite and delta-ferrite during sintering temperatures. Dilatometry experiments were conducted and followed by the data postprocessing for the model calibration. The calibrated model was incorporated in a FEM code and validated against experimental data from BJT sintered components, showing the remarkably accuracy of the numerical simulations, with small geometric deviations (0.56 mm) related to the assumption of isotropic shrinkage in the model proposed. In parallel, other alternative models were implemented based on different normalized bulk viscosity formulations, which underestimate/overestimate the sintered distortions.

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