电子探针
等温过程
电子背散射衍射
相(物质)
透射电子显微镜
衍射
三元运算
相图
大气温度范围
结晶学
分析化学(期刊)
电子衍射
扫描电子显微镜
化学
材料科学
热力学
微观结构
矿物学
光学
物理
纳米技术
复合材料
色谱法
有机化学
程序设计语言
计算机科学
作者
Shuai Xu,Junpin Lin,Yongfeng Liang,Jianping He,Yi Qiao,Limei Cha,Liang Yang,Xianquan Jiang
标识
DOI:10.1016/j.jallcom.2023.168758
摘要
This paper is a continuation of our recent publication [S. Xu, et al. Journal of Alloys and Compounds 900 (2022) 163399–163407]. We systematically characterized the diffusion multiples using scanning electron microscopy (SEM), electron probe microanalysis (EPMA), electron backscatter diffraction (EBSD), transmission Kikuchi diffraction (TKD) and transmission electron microscopy (TEM) and constructed the whole composition range of the 980 °C isothermal sections. The constructed range includes nine stable phases, twenty two-phase regions and ten three-phase regions at 980 °C. Six phase reactions occurring between 900 °C and 980 °C were determined. The ωo phase was formed by the βo+ γ→ωo reaction at a temperature just below 980 °C. The βo phase vanished through the βo→α2 + ωo+O reaction at a temperature just above 900 °C. These experimental results will bridge the existing research gap by providing the missing thermodynamic data. We believe that accurate predictions of phase diagrams and reactions occurring at intermediate temperatures using the obtained data are now feasible and the recomputations will resolve previous inconsistences and disputes.
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