葡聚糖
化学
柱色谱法
硅胶
色谱法
有机化学
酶
出处
期刊:Journal of Kunming Medical University
日期:2013-01-01
摘要
Objective To study the chemical compositions of Calocedrus macrolepis.Methods The chemical compositions were isolated with silica gel column chromatography,semi-preparative HPLC,Sephadex LH-20 and MPLC packed with MCI gel and their structures were elucidated on the basis of physical characteristics and spectral data.Results Five compounds were obtained,and their structures were identified as caryolane-1,9β-diol(1),eudesma-4(15)-ene-lβ,6α-diol(2),5-epi-eudesma-4(15)-ene-1β,6β-diol(3),eudesma-11(13)-ene-4β,9β-diol(4),coniferaldehyde(5).Conclusion All of these compounds are isolated from the Calocedrus macrolepis for the first time.
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