By using the pressureleaching solution of indiumcontaining zinc sulfide concentrate as raw material,the indiumiron separation process was studied by the method of reducing Fe~(3+),neutralizing,precipitating indium and extracting.The results showed that the reducing rate of Fe3+ was 91.5% for 180 minutes of reducing time at 90°C with the adding quantity of zinc sulfide concentrate 1.8 times as the theoretical need.The precipitating rate of indium reached 94.2% at the final pH 4.5,and the extracting rate of indium was 90% for 5 minutes of extracting time at 25°C.