材料科学
扫描电子显微镜
透射电子显微镜
双节点
薄脆饼
硅
薄膜
次级电子
膜
光电子学
复合材料
电子
分析化学(期刊)
光学
纳米技术
化学
生物化学
量子力学
探测器
光电倍增管
物理
色谱法
作者
Hong Chan,Violeta Prodanović,A.M.M.G. Theulings,T. ten Bruggencate,K. HAGEN,P.M. Sarro,H. V. D. Graaf
标识
DOI:10.1088/1748-0221/17/09/p09027
摘要
Abstract Large-area transmission dynodes were fabricated by depositing an ultra-thin continuous film on a silicon wafer with a 3-dimensional pattern. After removing the silicon, a corrugated membrane with enhanced mechanical properties was formed. Mechanical metamaterials, such as this corrugated membrane, are engineered to improve its strength and robustness, which allows it to span a larger surface in comparison to flat membranes while the film thickness remains constant. The ultra-thin film consists of three layers (Al 2 O 3 /TiN/Al 2 O 3 ) and is deposited by atomic layer deposition (ALD). The encapsulated TiN layer provides in-plane conductivity, which is needed to sustain secondary electron emission. Two types of corrugated membranes were fabricated: a hexagonal honeycomb and an octagonal pattern. The latter was designed to match the square pitch of a CMOS pixel chip. The transmission secondary electron yield was determined with a collector-based method using a scanning electron microscope. The highest transmission electron yield was measured on a membrane with an octagonal pattern. A yield of 2.15 was achieved for 3.15 keV incident electrons for an Al 2 O 3 /TiN/Al 2 O 3 tri-layer film with layer thicknesses of 10/5/15 nm. The variation in yield across the surface of the corrugated membrane was determined by constructing a yield map. The active surface for transmission secondary electron emission is near 100%, i.e. a primary electron generates transmission secondary electrons regardless of the point of impact on the corrugated membrane.
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