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Ultra-thin corrugated metamaterial film as large-area transmission dynode

材料科学 扫描电子显微镜 透射电子显微镜 双节点 薄脆饼 薄膜 次级电子 光电子学 复合材料 电子 分析化学(期刊) 光学 纳米技术 化学 生物化学 量子力学 探测器 光电倍增管 物理 色谱法
作者
Hong Chan,Violeta Prodanović,A.M.M.G. Theulings,T. ten Bruggencate,K. HAGEN,P.M. Sarro,H. V. D. Graaf
出处
期刊:Journal of Instrumentation [Institute of Physics]
卷期号:17 (09): P09027-P09027 被引量:1
标识
DOI:10.1088/1748-0221/17/09/p09027
摘要

Abstract Large-area transmission dynodes were fabricated by depositing an ultra-thin continuous film on a silicon wafer with a 3-dimensional pattern. After removing the silicon, a corrugated membrane with enhanced mechanical properties was formed. Mechanical metamaterials, such as this corrugated membrane, are engineered to improve its strength and robustness, which allows it to span a larger surface in comparison to flat membranes while the film thickness remains constant. The ultra-thin film consists of three layers (Al 2 O 3 /TiN/Al 2 O 3 ) and is deposited by atomic layer deposition (ALD). The encapsulated TiN layer provides in-plane conductivity, which is needed to sustain secondary electron emission. Two types of corrugated membranes were fabricated: a hexagonal honeycomb and an octagonal pattern. The latter was designed to match the square pitch of a CMOS pixel chip. The transmission secondary electron yield was determined with a collector-based method using a scanning electron microscope. The highest transmission electron yield was measured on a membrane with an octagonal pattern. A yield of 2.15 was achieved for 3.15 keV incident electrons for an Al 2 O 3 /TiN/Al 2 O 3 tri-layer film with layer thicknesses of 10/5/15 nm. The variation in yield across the surface of the corrugated membrane was determined by constructing a yield map. The active surface for transmission secondary electron emission is near 100%, i.e. a primary electron generates transmission secondary electrons regardless of the point of impact on the corrugated membrane.
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