Effect of Solution Temperature on the Microstructure Evolution and Tensile Properties of GH4175 Superalloy

材料科学 微观结构 高温合金 极限抗拉强度 延伸率 体积分数 碳化物 粒度 晶间断裂 脆性 溶解 冶金 复合材料 晶界 化学工程 工程类
作者
Zhigang Zhang,Jian Luo,Haokun Guo
出处
期刊:Lecture notes in mechanical engineering 卷期号:: 703-712
标识
DOI:10.1007/978-3-031-41341-4_74
摘要

In the present study, GH4175 superalloy was treated in the solution temperature range of 1100 ℃–1160 ℃ for 2 h, followed by unified aging treatment at 760 ℃ for 20 h. The microstructure of one step (only solution) and two-step (solution and age) treatment was compared to analyze the change of microstructure characteristics at different solution temperatures. The specimens after two-step treatment were subjected to tensile tests at 750 ℃, and corresponding fracture morphologies were observed to reveal the fracture behavior of GH4175 superalloy. The results show that the grain size of γ matrix increases from 4.6 μm to 6.8 μm as solution temperature increases from 1100 ℃ to 1140 ℃, but the volume fraction of primary γ´ particles decreases from 18.7% to 7.2%. The grain size of γ matrix significantly coarsens to 78.8 μm after solution treatment at 1160 ℃ because the dissolution of primary γ´ particles weakens the pinning effect. The secondary γ´ particles are refined after two-step treatment. An optimal yield strength of 1166 MPa is obtained by solution treatment at 1140 ℃ for 2 h followed by aging at 760 ℃ for 20 h. The re-precipitated secondary γ´ particles of GH4175 provide the major strengthening effect. However, as the solution temperature increases to 1160 ℃, the yield strength and elongation decrease to 1049 MPa and 2.88% respectively, which is attributed to the combined brittle intergranular fracture effect of coarsen γ grains and the distribution of undissolved carbides.
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