微晶纤维素
水解
纤维素
蒸馏水
色谱法
酸水解
微晶
化学
还原糖
高效液相色谱法
材料科学
糖
有机化学
结晶学
作者
Bo Yuan,Ying Wang,Ying Ji,Qiu-Hong Wang
出处
期刊:Advanced Materials Research
[Trans Tech Publications]
日期:2013-08-30
卷期号:750-752: 1626-1629
标识
DOI:10.4028/www.scientific.net/amr.750-752.1626
摘要
In this paper, plasma acid was obtained by treating distilled water with dielectric barrier discharge at atmospheric pressure in order to hydrolyze cellulose. The acidity of plasma acid was studied through a single factor experiment. A plasma acid with pH value of 1.42 was obtained and used to hydrolyze microcrystalline cellulose at 80°C for 60min. Under this condition, the integrated optical density (IOD) of the hydrolysis sample was 0.589. Based on standard glucose curve, the total reducing sugar (TRS) was calculated to be 53.75mg and the TRS yield was 53.75%. The filtrate was evaporated to get the solid hydrolysis sample to be analyzed by High-performance liquid chromatography (HPLC). The results showed that the sample mainly consisted of glucose, which proved that microcrystalline cellulose could be hydrolyzed by plasma acid. Therefore, it could be concluded that it was an environmentally friendly and economical method to hydrolyze the microcrystalline cellulose by plasma acid.
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