化学
苯丙素
糖苷
酰胺
葡萄糖苷
葡聚糖
色谱法
罂粟科
立体化学
高效液相色谱法
有机化学
生物碱
生物合成
医学
替代医学
病理
酶
作者
Hui-Na Yao,Hang Zhang,Wen‐Xuan Wang,Ni-Li Zan,Di‐Fa Liu,Yunfang Zhao,Jiao Zheng,Pengfei Tu,Jun Li
出处
期刊:PubMed
[National Institutes of Health]
日期:2020-05-01
卷期号:45 (10): 2411-2416
被引量:2
标识
DOI:10.19540/j.cnki.cjcmm.20200220.202
摘要
Two new phenylpropanoid amide glycosides and ten analogues were isolated from the CH_2Cl_2 layer of 95% ethanol extract of the whole plants of Corydalis racemosa by using various chromatographic techniques, including silica gel, Sephadex LH-20, ODS column chromatographies, and semi-preparative HPLC. Their structures were identified on the basis of physicochemical properties, MS, NMR, and IR spectroscopic data as N-cis-sinapoyltyramine-4'-O-β-glucoside(1), N-cis-sinapoyl-3-methoxytyramine-4'-O-β-glucoside(2), N-cis-sinapoyltyramine(3), N-cis-feruloyltyramine(4), N-trans-cinnamoyltyramine(5), N-trans-feruloylphenethylamine(6), N-trans-p-methoxycinnamoyl-3-hydoxyoctopamine(7), N-cis-feruloyl-3-methoxytyramine(8), N-trans-feruloyltyramine(9), N-trans-feruloyl-3-methoxytyramine(10), N-trans-sinapoyltyramine(11), and N-trans-p-coumaroyltyramine(12). Compounds 1 and 2 are new compounds. Compounds 3-7 are obtained from the plants of Papaveraceae for the first time, and compounds 8-12 are firstly isolated from C. racemosa.
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