材料科学
烧结
氮化硅
陶瓷
超短脉冲
微观结构
氧化物
相(物质)
复合材料
冶金
硅
氮化物
激光器
光学
有机化学
化学
物理
图层(电子)
作者
Rui-Hao Luo,Milad Kermani,Zhaoliang Guo,Jin‐Yong Dong,Chunfeng Hu,Fei Zuo,Salvatore Grasso,Beibei Jiang,Guanglin Nie,Zheng-Qing Yan,Qiang Wang,Yanling Gan,Fupo He,Hua‐Tay Lin
标识
DOI:10.1016/j.jeurceramsoc.2021.06.021
摘要
Ultrafast High-temperature Sintering (UHS) has been successfully applied to fabricate the silicon nitride (Si3N4) bulks, as the first attempt of ultra-rapid consolidation of a non-oxide ceramics. At a heating rate of 875 °C/min, the bulk Si3N4 ceramic with a relative density greater than 96 % and an α-β phase transformation degree above 80 % could be obtained within 300 s. The effects of ultrafast heating on the liquid phase sintering (LPS) were also comparatively studied. Results showed that, the ultrafast heating rate and high temperature under UHS might promote the LPS system evolving to a nonequilibrium state. By comparing with other pressureless sintering processes with much lower heating rates, UHS apart from reducing the processing time, and it is also an effective method to form a bimodal microstructure composed of interlocked rod-like β-Si3N4 grains.
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