铋
材料科学
透射电子显微镜
热分解
氢氧化物
粒径
纳米颗粒
氧化物
分解
化学工程
粒子(生态学)
粉末衍射
Crystal(编程语言)
核化学
无机化学
纳米技术
结晶学
冶金
有机化学
化学
程序设计语言
海洋学
地质学
计算机科学
工程类
作者
M.M. Patil,Vasanti Deshpande,Sanjay R. Dhage,V. Ravi
标识
DOI:10.1016/j.matlet.2005.03.037
摘要
A simple gel to crystal conversion route has been followed for the preparation of ultrafine Bi2O3 particles at 80–100 °C under refluxing conditions. Freshly prepared bismuth hydroxide gel is allowed to crystallize under refluxing and stirring conditions for 6–12 h. Formation of nanocrystallites of Bi2O3 is confirmed by X-ray diffraction (XRD) study. The thermal decomposition of bismuth hydroxide yields Bi2O3 only at 400 °C. This shows the advantage of the present method. Transmission electron microscope (TEM) investigations revealed that the average particle size is 50 nm for these oven-dried powders.
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