We report x-ray photoemission spectra for a 13% glass-filled nylon 6,6 polymer (PA66). XPS spectra were acquired with a SSI model SSX-100 instrument using monochromated Al Kα x-rays. We present the survey spectrum (binding energy 0–1000 eV) and a narrow spectrum of the C 1s, O 1s, and N 1s photoelectron peaks.