磁铁
分光计
材料科学
哈尔巴赫阵列
磁场
同质性(统计学)
核磁共振
场强
机械工程
物理
计算机科学
光学
工程类
量子力学
机器学习
作者
Peng Yu,Yanliang Xu,Zhongyi Wu,Yan Chang,Qiaoyan Chen,Xiaodong Yang
标识
DOI:10.1016/j.jmr.2018.07.014
摘要
The objective of this work is to develop a low-cost compact desktop NMR system based on Halbach magnets with the advantages of small size and ability to generate relatively high field strength. Considering the cost of manufacturing and assembling the magnetic blocks, the system utilized a 3-layer Halbach magnet and a wedge-shaped mechanical structure, which was designed for magnet rapid assembling. The comparison between simulation and calculation results of the initial magnetic field strength distribution showed that design theory and practice were in accordance. The initial homogeneity was 576 ppm in a square with a length of 5 mm. After passive shimming with two magnetic blocks and steel pieces, the uniformity reached 120 ppm in the same area. We developed and tested a compact single board spectrometer with digital modulation and demodulation in order to enhance the system mobility and improve the SNR. A self-made probe was used to carry out experiments with the spectrometer, and the spectral width at half-height reached 20 ppm in a cylinder with a diameter of 1.5 mm and a length of 1 mm. Compact structure and low cost of the system will facilitate and extend the application of desktop NMR system.
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