甲基丙烯酸
热重分析
共聚物
单体
高分子化学
离子液体
材料科学
纳米复合材料
傅里叶变换红外光谱
化学工程
聚合物
化学
有机化学
纳米技术
复合材料
催化作用
工程类
作者
Fatemeh Bazmi Zeynabad,Abdolrahim Abbaszad Rafi,Mehrdad Mahkam,Hossein Taheri
标识
DOI:10.1080/03602559.2016.1163596
摘要
New pH-sensitive polymer–clay nanocomposites were prepared through in situ copolymerization of methacrylic acid with modified laponite. First, an ionic liquid monomer, 1-(4-vinylbenzyl)-3-methylimidazoliumchloride, was synthesized through the quaternization of N-methylimidazole with 4-vinylbenzylchloride. Then, the ionic liquid monomer was intercalated between the laponite layers by the ion-exchange reaction and subsequently copolymerized with methacrylic acid. The composites were characterized by Fourier transform infrared spectroscopy, X-ray diffraction, thermogravimetric analysis, energy-dispersive X-ray spectroscopy (EDX), and scanning electron microscopy to study their structure and the role, laponite plays. Naproxen, was entrapped into these pH-sensitive nanocarriers and the in vitro release profiles were established separately in both enzyme-free simulated gastric and colonic fluids.
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