漫反射红外傅里叶变换
表征(材料科学)
粉末衍射
光谱学
金属有机骨架
傅里叶变换红外光谱
红外光谱学
扫描电子显微镜
材料科学
纳米技术
化学工程
化学
分析化学(期刊)
有机化学
物理化学
结晶学
光催化
吸附
催化作用
物理
工程类
复合材料
量子力学
作者
Ashlee J. Howarth,Aaron W. Peters,Nicolaas A. Vermeulen,Timothy C. Wang,Joseph T. Hupp,Omar K. Farha
标识
DOI:10.1021/acs.chemmater.6b02626
摘要
Metal–organic frameworks (MOFs) are structurally diverse materials comprised of inorganic and organic components. As the rapidly expanding field of MOF research has demonstrated, these materials are being explored for a wide variety of potential applications. In this tutorial review, we give an overview of the current best practices associated with the synthesis, activation, and characterization of MOFs. Methods described include supercritical CO2 activation, single crystal X-ray diffraction (XRD), powder X-ray diffraction (PXRD), nitrogen adsorption/desorption isotherms, surface area calculations, aqueous stability tests, scanning electron microscopy (SEM), inductively coupled plasma optical emission spectroscopy (ICP-OES), nuclear magnetic resonance spectroscopy (NMR), and diffuse reflectance infrared Fourier transform spectroscopy (DRIFTS). A variety of different MOFs are presented to aid in the discussion of relevant techniques. In addition, some sections are accompanied by instructional videos to give further insight into the techniques, including tips, tricks, and suggestions only those at the bench could describe.
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