Microstructure and Mechanical Properties of Polyacrylonitrile Precursor Fiber with Dry and Wet Drawing Process

Polyacrylonitrile (PAN) fibers are typically used as precursor fibers for carbon fiber production, produced through wet-spinning processes. The drawing process of the spun fiber can be classified into dry and wet drawing processes. It is known that the drawing stability and stretching ratio differ depending on the drawing process; however, the elementary characteristics are approximately similar. In this study, the mechanical properties of PAN fibers have been examined based on these two drawing processes with the differences analyzed through the analysis of microstructures. Further, to examine the composition of the fiber, element analysis has been conducted, and thereafter, the microstructure of the fiber is examined through X-ray diffraction analysis. Finally, the characteristics of PAN fibers and its mechanical properties has been examined according to each drawing condition. There are differences in moisture content and microstructure according to the drawing process, and it affects the tensile behavior. The results obtained could have potential implications if the processes are combined, as it could result in a design for a stable and highly efficient drawing process.