材料科学
热液循环
扫描电子显微镜
拉曼光谱
光致发光
相(物质)
化学工程
六角相
纳米颗粒
衍射
能量色散X射线光谱学
粉末衍射
纳米棒
纳米技术
六方晶系
分析化学(期刊)
结晶学
复合材料
光学
光电子学
色谱法
有机化学
化学
工程类
物理
作者
Xin Hou,Peitao Xie,Shaolin Xue,Hange Feng,Lingwei Li,Zhiyuan Liu,Rujia Zou
标识
DOI:10.1016/j.mssp.2018.01.023
摘要
In this study, CuSe nanoplates have been synthesized using copper sulfate and Se powder as the raw materials by a simple and rapid hydrothermal process. The edta disodium (EDTA) was used as the surface active agent to moderate the morphologies of CuSe nanoparticles. As-synthesized CuSe samples were successfully characterized by X-ray diffraction (XRD), X-ray energy dispersive spectroscope (EDS), scanning electron microscopy (SEM) and Raman spectrometer, UV–visible (UV–vis) spectroscopy and photoluminescence (PL). XRD analysis demonstrated the hexagonal klockmannite phase of CuSe nanoplates. The as-synthesized products were homogeneous and highly crystallized. The structural and compositional analysis revealed that the products were the pure phase of CuSe with corresponding atomic ratios. With sufficient reaction materials, the reaction time has an influence on the growth of large-scale CuSe nanoplates. CuSe nanoplates obtained by the described method could be a potential material in photoelectric device.
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