Effect of inert glass on the physical and mechanical properties of zirconia dental ceramics fabricated by digital light processing

立方氧化锆 材料科学 惰性 陶瓷 牙科陶瓷 复合材料 牙瓷 矿物学 化学 有机化学
作者
Faqiang Zhang,Kesheng Zhang,Yangbo Zuo,Xia Jin,Jingzhou Yang
出处
期刊:Journal of the American Ceramic Society [Wiley]
卷期号:107 (7): 4689-4704 被引量:2
标识
DOI:10.1111/jace.19793
摘要

Abstract Zirconia dental ceramics incorporated with inert dental glass (IDG) were fabricated by digital light processing (DLP). The effects of the amount of added IDG on the physical properties and microstructure of sintered samples were investigated. Highly dense zirconia dental ceramic samples with a relative density of 98.9% were obtained by adding different amounts of IDG sintered at 1500°C. With the addition of 1 wt% IDG, the Vickers hardness, fracture toughness, and wear resistance increased to 13.03 GPa, 6.33 MPa m 1/2 , and 0.03 mg/(mm 2 min), respectively. However, with the incremental addition of IDG at 3 and 5 wt%, a slight reduction in Vickers hardness, fracture toughness, and wear resistance was observed. The values recorded were 12.68 GPa, 5.90 MPa m 1/2 , and 0.05 mg/(mm 2 min) for the former, and 11.86 GPa, 5.48 MPa m 1/2 , and 0.06 mg/(mm 2 min) for the latter. Scanning electron microscopy observation suggested that 1 wt% IDG incorporated into zirconia dental ceramic samples resulted in an optimal microstructure, with IDG existing at triple junctions of zirconia grains to form a discrete secondary phase. The broken surface revealed transgranular fracture features. This investigation indicates that adding a proper amount of IDG is an effective method to enhance the properties of DLP‐fabricated zirconia dental ceramics.
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