中间相
材料科学
过滤(数学)
碳纤维
石油焦
复合材料
石油
化学工程
有机化学
化学
焦炭
冶金
液晶
光电子学
复合数
统计
数学
工程类
作者
Enrique Sánchez Mora,Clara Blanco,Ricardo Santamarı́a,Marcos Granda,Rosa Menéndez
出处
期刊:Carbon
[Elsevier]
日期:2003-01-01
卷期号:41 (3): 445-452
被引量:42
标识
DOI:10.1016/s0008-6223(02)00354-8
摘要
This paper studies a novel method for the preparation of mesophase pitches suitable as carbon fibre precursors. A series of thermally treated petroleum pitches with mesophase contents ranging from 10.8 to 52.2 vol.% was obtained from pitch A-240. Separation of the phases was initially attempted by hot filtration, a suitable method for separating the phases in thermally treated coal-tar pitches. Although filtration failed for the petroleum samples, the behaviour observed led to the development of a new separation method that consists in the sedimentation of the mesophase. This method, after optimisation, yielded pitches with mesophase contents up to 97 vol.%, which were easily spun into carbon fibres of reasonable mechanical properties.
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