The dielectric barrier discharge‐based non‐thermal plasma technique is one of the most prominent techniques which give peerless results in controlling the concentration of NO X . However, when it comes to the automobile diesel engine, availability of high‐voltage pulse power supply is the major constraint. In this study, battery‐powered high‐voltage pulse power supply for NO X treatment has been proposed. Two types of electrodes: rod type and rod with helical spring type are studied for the treatment of exhaust. Cascaded plasma‐adsorbent technique has also been used to enhance NO X removal efficiency. Experiments have been conducted with two different gas flow rates, i.e. 4 l and 6 l/min at laboratory level and have got significant results toward removal of NO X . When the exhaust has been treated with plasma alone, the reactor with rod‐type electrode has shown 85% NO X removal efficiency at a specific energy (SE) of 283 J/l with a flow rate of 4 l/min. When the plasma reactor is cascaded with the adsorbent reactor, both adsorbents: 13x molecular sieve (MS13x) and activated alumina are able to remove 100% of NO X with the proposed power supply at a lesser SE.