材料科学
液化
磁铁
磁场
超导磁体
显微镜
热的
量子隧道
制作
光电子学
扫描隧道显微镜
电流(流体)
低温学
超导电性
核工程
超高真空
温度测量
基础(拓扑)
领域(数学)
光学
水冷
核磁共振
温度控制
光学显微镜
复合材料
低温恒温器
扫描电子显微镜
磁强计
凝聚态物理
混合(物理)
磁性
作者
Ruisong Ma,Yuanzhi Huang,Guangyuan Han,Hao Li,Chenshuai Shi,Fan Wang,X H Yu,Songping He,Dairong Liu,Li Liu,Shesong Huang,Hong-Jun Gao,Qing Huan
摘要
We have developed a cryogen-free ultra-low temperature scanning tunneling microscope (STM) system based on remote liquefaction technology. Integrated with a cryogen-free room-temperature bore 5 T superconducting magnet, the system achieves continuous and stable operation in the sub-Kelvin and high magnetic field regime. A two-stage 4He circulation (∼20 and ∼2 K) precools a continuous-flow STM insert, after which another circulation loop, filled with either 3He or 4He, is liquefied and further cooled by evaporative pumping. The sample stage reaches base temperatures of 420 mK (4He-3He mode) and 894 mK (4He-4He mode). The temperature fluctuations of approximately ±0.1 mK are achieved at 500 mK and 1 K under proportional-integral-derivative control. Characterization, including cooling curves, current noise, thermal drift, atomic-resolution imaging, and variable-temperature/magnetic-field spectroscopy, demonstrates the performance comparable to conventional liquid-4He bath-based STM systems in terms of resolution, stability, and tunability. Furthermore, the system enables a months-long continuous operation across a wide temperature range, featuring straightforward magnet upgradability, direct high-temperature baking capability, and compactness with low installation requirements. This cryogen-free design provides a viable approach for other vibration-sensitive, high-precision experiments requiring long-term continuous operation under extreme conditions.
科研通智能强力驱动
Strongly Powered by AbleSci AI