化学
联氨(抗抑郁剂)
芳基
冷凝
缩醛
微波食品加热
二甲基甲酰胺
微波加热
有机化学
组合化学
色谱法
量子力学
热力学
物理
烷基
溶剂
作者
A.-K. Pleier,Holger Glas,M. Grosche,Peter Sirsch,Werner R. Thiel
出处
期刊:Synthesis
[Thieme Medical Publishers (Germany)]
日期:2001-01-01
卷期号:2001 (01): 0055-0062
被引量:88
摘要
Condensation of aromatic acyl compounds with N,N-dimethylformamide diethyl acetal in a pressure tube under microwave heating gives 1-aryl-3-dimethylaminoprop-2-enones in almost quantitative yields. In the presence of hydrazine, these intermediates are transferred to the corresponding 3-arylpyrazoles.
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