Seith has already published his study on the solid solubility of Ag in Pb. According to his results, the solid solubility is 0.1% Ag at the eutectic temperature (304°). We ascertained not only Seith’s results, but examined the solubility behavior in the lower temperature range than 200° in which he had not obtained exact values.According to the author’s experiment, the solid solubility did not change linearly, for example, at 180°, 0.04% Ag, 108°, 0.025% Ag and 78°, 0.01% Ag.For the determination of the solubility limit, the following experimental means were applied: (a) The measurment of electric resistance. (b) Differential thermal analysis. (c) Hardness test. (d) Thermal analysis. (e) X-ray analysis.