纳米棒
锌
纤锌矿晶体结构
光致发光
材料科学
热重分析
氢氧化锌
透射电子显微镜
傅里叶变换红外光谱
氢氧化钠
无机化学
氧化物
化学工程
核化学
化学
纳米技术
物理化学
光电子学
工程类
冶金
作者
Virendra Prasad,Charlene P D'Souza,Deepti Yadav,A. J. Shaikh,N. Vigneshwaran
标识
DOI:10.1016/j.saa.2005.10.001
摘要
Well-crystallized zinc oxide nanorods have been fabricated by single step solid-state reaction using zinc acetate and sodium hydroxide, at room temperature. The sodium lauryl sulfate (SLS) stabilized zinc oxide nanorods were characterized by using X-ray diffraction, Fourier transform infrared spectroscopy, transmission electron microscopy and photoluminescence spectroscopy. The X-ray diffraction revealed the wurtzite structure of zinc oxide. The size estimation by XRD and TEM confirmed that the ZnO nanorods are made of single crystals. The growth of zinc oxide crystals into rod shape was found to be closely related to its hexagonal nature. The mass ratio of SLS:ZnO in the nanorods was found to be 1:10 based on the thermogravimetric analysis. Blue shift of photoluminescence emission was noticed in the ZnO nanorods when compared to that of ZnO bulk. FT-IR analysis confirmed the binding of SLS with ZnO nanorods. Apart from ease of preparation, this method has the advantage of eco-friendliness since the solvent and other harmful chemicals were eliminated in the synthesis protocol.
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