傅里叶变换红外光谱
透射电子显微镜
铁
赤铁矿
微晶
分析化学(期刊)
扫描电子显微镜
吸附
材料科学
矿物学
核化学
化学
化学工程
无机化学
结晶学
纳米技术
物理化学
色谱法
工程类
复合材料
作者
Yiqun Xu,Ming Yang,Chengda He,Huixin Xiong
出处
期刊:PubMed
日期:2013-12-01
卷期号:33 (12): 3330-3
被引量:4
摘要
In the present work, based on the stable phase of alpha-FeOOH and beta-FeOOH easily formed in ferric solutions of Fe (NO3)3 and FeCl3 at the appropriate pH values, respectively, the phase and crystallizability, morphologies and sizes for the particles of FeOOH minerals prepared under the conditions of heating at 40 and 70 degreeC, and magnetic stirring at 25 degreeC were identified and examined by X-ray diffraction (XRD), transmission/scanning electron microscopy (TEM/SEM) and laser scattering particle analyzer. Meanwhile the surface chemistry properties were also detected and analyzed by Fourier transform infrared spectrometer (FTIR). Investigation results showed that the prepared minerals Gth-T70 (alpha-FeOOH), Aka-T40 and Aka-T70 (beta-FeOOH) have good properties of nanocrystallity, homogeneous particles and higher specific surface areas, which induced that the above alpha, beta-FeOOH are potentially excellent adsorbent materials for removal of some contaminants in circumstances.
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