纤锌矿晶体结构
纳米棒
X射线光电子能谱
锌
硝酸锌
吸附
材料科学
玫瑰花结(裂殖体外观)
氢氧化物
化学
透射电子显微镜
纳米结构
无机化学
分析化学(期刊)
化学工程
结晶学
六方晶系
纳米技术
物理化学
有机化学
免疫学
工程类
生物
作者
Rizwan Wahab,S. G. Ansari,Hyung‐Kee Seo,Young Soon Kim,Eun‐Kyung Suh,Hyung‐Shik Shin
标识
DOI:10.1016/j.solidstatesciences.2008.07.009
摘要
Rosette-like structures of ZnO were synthesized at low temperature (60 °C) using solution process over 20 min of time. Hydroxylamine hydrochloride was used as capping agent with zinc nitrate hexahydrate and sodium hydroxide. Transition from triangular shaped plate like particles to rosette-like structure and to individual nanorods is observed with increasing refluxing temperature. Single-crystalline nature with wurtzite hexagonal phase is confirmed from transmission electron microscopic observations. Photoelectron spectroscopic measurement presented spectra close to the standard bulk ZnO, with an O 1s peak composed of surface adsorbed O–H group, O2− in the oxygen vacancies on ZnO structure and ZnO.
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